水滑石与氢氧化镁纳米晶的液相法制备及其生成机制

研究了纳米晶镁铝水滑石Mg6Al2(OH)16CO3·4H2O与 Mg(OH)2 的液相法制备及其物相变化.X射线衍射(XRD)和透射电镜(TEM)分析表明,在制备温度分别为30 ℃的低温和190 ℃的高温,可获得纯度大于99%的氢氧化镁针状纳米晶,在45~150 ℃的中间温度范围,可获得纯度大于 99%的镁铝水滑石针状纳米晶.合成温度由35 ℃提高到45 ℃时,生成物相由氢氧化镁变成镁铝水滑石相;合成温度由 170 ℃提高到190 ℃时,生成物相由镁铝水滑石相变成氢氧化镁相.提出低温时生成物的变化与瞬间生成无定形态的Mg(OH)2 有关,无定形态的Mg(OH)2 沉淀为Al13(OH)7 32 中铝离子以及CO2-3 扩散进入Mg(OH)2提供了更为有利的条件.高温时生成物的变化,是由于温度的升高,使含结晶水的镁铝水滑石纳米晶中间层中的高极性水分子堆积所要求的一定的物理条件受到破坏所致.     

"核心刊物"闹剧应当休矣--论"核心刊物"闹剧的实质与危害

“核心刊物”闹剧在我国愈演愈烈，在社会上产生了严重影响。作者对“核心刊物”闹剧的表象进行了描述，并对其实质和危害进行了分析。认为“核心刊物”闹剧是名利作祟，学术腐败的温床；极大地损害了我国期刊界的形象，腐蚀了我国期刊界的肌体，是我国现代化建设中的一大隐患。如此下去，我们期刊界无法面对国人，也无法在世界面前立足，最终必将自食苦果。期刊界、学术界也应打假，制止“核心刊物”闹剧已刻不容缓。国家期刊管理部门应出台政策和措施，制止“核心刊物”闹剧恶性发展，恢复核心刊物的庄严面目。现行的职称评定机制与“核心刊物”闹剧是一对孪生姊妹，也必须进行治理。应当整顿职称评定中的不良倾向，推行职称聘任制，打破职称终身制的局面。     

红外遥控预付费水表的设计

针对IC卡水表应用于工业环境时存在的不足之处，提出了一种基于红外遥控的预付费水表的设计方案。从上位PC机通信电路、红外发送与接收电路以及电源模块等几个方面详细介绍了该水表系统硬件部分的实现方法。此外简要介绍了系统的软件设计以及红外通信硬件抗干扰措施。     

高离化态Cu的光谱分析

利用束箔光谱技术研究HI—13串列加速器提供的能量为80MeV和110MeV的Cu束与靶室中的碳膜碰撞激发光谱的情况。     

一类二阶奇异边值问题的正解

证明了一类与一阶导数x有关的二阶奇异边值问题正解的存在性，这里的奇异问题是指在x=0和x′＝0是奇异的。     

水泥厂设备管理多层分布系统及优化设计的实现

作者研究了水泥厂设备管理多层分布系统结构的设计及其良好扩展性的实现，重点针对一般MIS系统忽视效益的弊病，建立了一种设备优化管理的平台，该平台可使企业提高管理效益．     

FPGA／CPLD可编程逻辑器件的在系统配置方法

讨论了基于SRAM技术的CPLD／FPCA可编程逻辑器件的编程方法，并以ALTERA公司FLEX10系列器件为例，提出了一种利用微处理器对可编程逻辑器件进行在系统多方案配置的实用方法。该方法成本低廉、简单易行，能在系统复位或上电时自动对器件编程，不仅有效的解决了基于SRAM的CPLD／FPGA器件掉电易失性的问题，而且使单一芯片可以具有多种逻辑功能，实现了该类器件逻辑功能的在系统多方案的灵活配置。     

Lightning activity on the central Tibetan Plateau and its response to convective available potential energy

Lightning flash activities on the central Tibetan Plateau have been studied by using the satellite-based Lightning Imaging Sensor(LIS)database from January 1998 to July 2002.The lightning activity shows a clear diurnal variation on the central Plateau.The peak lightning activity appears at about 17:00 which is 3 h earlier than that in Jingxhou,Hubei in the same latitude belt nearby,indicating that the lightning activity is a sensitive indicator of solar heating on the Plateau.The lightning discharge is weaker on the Plateau than Jingzhou.Hubei and other low-altitude continental regions because of the lower convective available potential energy(CAPE)on the Plateau.The CAPE on the Plateau is 12 times lower than that in Jingzhou,Hubei,and 20 times lower than that in the sea-level region,such as Guangzhou and Florida.However,the sensitivity of lightning activity to CAPE changes on the Plateau is up to 30 times more sensitive than other prominent low-altitude regions.     

C－isotope composition and significance of the Sinian on the Tarim plate

102 samples of limestones,mudrocks shales and tillites from the Sinian in Kuluketage have been analyzed ,Four formations in the Sinian belong to glacial deposits in which the differences in δ^13C are distinct (-14.7‰- 4.2‰),Distinctly negative δ^13C excursions for three times support the viwe of three glacial deposits in this area suggested by previous authors,except for the durations of them ,δ^13C values are generally positive in the Beiyixi Formation of lower part of the Lower Sinian ,representing probably the rock records of a continental rift related to break-up of the Rodinian supercontinent,There are three times of distinct excursions of δ^13C curve in all strata,The first one is from positive values at the bottom to about -5‰ at the top of the Beiyixi Formation ,The second one,from 0‰-3‰ in the Arletonggou Formation of upper part of the Lower Sinian to -3.4‰---14.4‰ in the Teruiaiken Formation.The third one,from positive values in the Zhamoketi Formation of lower part of the Upper Sinian to negative values in glacial varves at the top of the Hankeerqiaoke Formation.     

A new Euprox from the Late Miocene of Yuanmou,Yunnan Province,China,with interpretation of its paleoenvironment

The Yuanmou Basin of Yunnan Province is a hotspot for the research of early homind evolution and its environmental background.During the implementation of the Program“Research of the Origin and Evolution of Early Man and Its Environmental Baqckground” from 1998 to 2001,a huge quantity of hominoid and mammal fossils were collected.The present report systematically describes an Euprox robustus sp.nov.identified during the recent laboratory work on the collected material.Euprox is a group of earliest cervids with true antlers.The new species is the third one of the genus discovered in China.Judged by its morphologic characteristics,the new species feed on juicy and tender leaves of dicotyledon.It implies that the vegetation of its epoch in the Yuanmou Basin is a kind of southern subtropical evergreen forest and the climate is humid and temperate with evident seasonality.The latter is mostly influenced by the monsoon and secondly by the latitude.